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Lyophilized powder freezes fine for long-term storage, but once a peptide is in solution, ice crystals physically damage the structure you lose potency and get precipitation on thaw

LUPKIN: And what Chris saw, big picture, on his tour of these pharmacies was how quickly and nimbly they were able to expand their operations to meet this deluge of demand

In Annals of Pharmacotherapy

The mixed solution was stirred at room temperature for 24 h and the precipitate was collected by centrifugation at 12000 rpm for 10 min, followed by gently washing 3 times with DI water to remove the free BSO

As soon as they get what they thought they wanted, they always want more