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The reduction of the azido group was performed twice in a mixture of 1,4-dioxane/H 2 O (7:3 v/v) (5 mL) with a 1 M PMe 3 solution in THF (10 equiv) under microwave irradiation (50 C, 50 W, 30 min)

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After about a year without treatment with semaglutide, net weight loss was down to 5.5%

(2021, May 25)